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ICP5000 Dual View Indu...

CP5000DV Dual View Inductively Coupled Plasma
Optical Emission Spectrometer (ICP-OES) – Technical Presentation.
Introduction to PG Instruments Limited Scientific Instruments – Development Leader
PG Instruments Limited is a British company that has for many years manufactured a comprehensive range of UV-Visible
Spectrophotometers and Atomic Absorption Spectrometers. Based near Leicester in the heart of the UK we export to almost
every country in the world. Over the last few years PG Instruments has diversified and considerably added to our portfolio of
instrumentation. In addition to the UV-Vis Spectrophotometers and Atomic Absorption Spectrometer instruments we also
produce Water Purifiers, Micro-Wave Digestion Systems, Atomic Fluorescence, Flame Photometers, pH and Conductivity
Meters, Automatic Titration, Karl Fischer Analysis Systems, etc. In 2016 we introduced an Inductively Coupled Plasma
Spectrometer system (ICP-OES), with just a Radial View and added the Dual View system to our comprehensive range of
analytical instruments at the end of 2016. The ICP5000DV is already installed in a number of laboratories. In the UK we have
sold to Rolls Royce Limited, The Waste Water Care Group, Churchill Group, Heineken Brewery, Wear Check Oil Analysis,
We have also units installed at Nestle in France, Belgium, Mexico, India, Peru, South Africa, Spain, and Italy to name but a
few
Due to its versatility and high performance, the instrument can be used in almost any laboratory for a wide range of
applications such as:
• Agricultural
• Food
• Geological
• Clinical
• Metal
• Petrochemical
• Environmental
• Mining
• Pharmaceutical
• Education

Description

S p e c i f i c a t i o n s
RF Generator
Generator Solid State (low voltage), maintenance free
RF Frequency 27.12MHz
Output Power Range 500 – 1600 Watts
Output Power Control Automatic
Output power steps. 10W max, PC adjustable
Output Power (RF) Stability <0.1%
Power Adjustment Time
Time to adjust power to sample impedance change is dependent on the sample. Matrix. For example it will take
longer for the matching network to adjust for sea waters to 30% Brine solutions. Typically the impedance change
is controlled in under 1 second.
Plasma Power Efficiency better than 75%
RF Coil Cooling Water Cooled
Plasma Coil cooling Water Cooled
Optical System
Grating Echelle Grating approx. 50 grooves/mm
Prism Cross Dispersion Device
Focal Length 400mm
Temperature Control 38˚C
Detector CCD (Charged Coupled Device)
Pixel Size 24µm x 24µm
Detector Pixels 1024 x 1024 pixels
Protection Anti-Blooming
Detector Cooling Triple Peltier Device
Wavelength Range 160nm – 870nm
Resolution 0.006nm @200nm
Purge Spectrometer and optical path
Optical View Radial and Axial simultaneously
Optical Height Adjustable via Software
Sample Introduction
Torches Demountable Self Aligning Totch is supplies as Standard
Spray Chambers Cyclonic Glass (standard)
Programmable Temperature Controlled (Optional)
Nebulizers Glass Concentric (standard)
Quartz Concentric (optional)
V-Groove (optional)
HF resistant (optional)
Sea Spray (optional)
Sample Intake 4 Channel system 12 Roller Peristaltic Pump (optional)
Sample Intake Hydride generation system, Continuous Flow (optional)
HF resistant
Optional
Auto-Sampler
Samples
Random Access type. Interface & software included. (optional)
Up to 360x8ml, 240x15ml, 160x20ml, 96x30ml, 84x50ml

14
Standards 10
• Rinse station Standard
• Dilution System Optional
Computer
Operating System Windows 10 Professional
Operation Control
The system has full control, of
the while system, keeping track
of and constantly monitoring:
The system is constantly
monitoring the RF Power,
forward and reflected, Gas
Flows and Pressures, Safety
System (see Picture below)
Flow of cooling water
Closing of the door and sample chamber
Plasma stability
Gas pressures
Gas flows
Axial or radial plasma view
Plasma ignition and shut-down
Safety system
Full function monitoring
Automatic sampling
Software
Operating Software ICP-Win Software
Element Library >70000 Spectral Lines showing inter-element corrections (IEC’s) and interferences.
Element Corrections IEC (inter-element corrections) and Background Corrections
Software Capabilities
• Multi–window and multi-method analysis program for fast simultaneous measurements.
• Built-in library of over 70,000 spectral lines
• Display of Visual Background correction points
• Display of complete “Spectrograms” showing automatically and manually calibrated spectral lines
• Permission of Management
• Password Change
• Check of instrument status
It includes RF power, cooling water pressure, Ar storage pressure, cooling
gas, auxiliary gas, carrier gas and the peristaltic pump operation condition
• Instrument Parameter Settings
• Settings of Detector
• Automatic Wavelength Calibration
• Manual wavelength calibration
• Torch Collimation
• Pump Speed Optimization
• Carrier gas optimization
• Creating a test
• Creating a new test
• Copy of a Stored Analysis Method
• Analysis and Data Processing
• Sample Analysis
• Background Matting & Peak Position Setting
• Recalculation of Results
• Editing of Calibration Curve
• Results Print and Data Export
• Pre-stored methods.
• Full control of the whole system (gas flows, axial or radial plasma view, plasma ignition and shut-down,
plasma stability, water flow, safety system, full function monitoring) and automatic sampling.
• Background correction either by the user or automatically, to achieve correction with optimal accuracy
and repeatability
• Calibration procedures, with external polynomial standards and with standard additions.
• Quality control program in accordance with the user’s choices and current international requirements.
• Presentation of the calibration curves and the peaks of all the analyzed items at the same time.
• HELP and SERVICE DIAGNOSTICS systems.
• Simultaneous reading of Background and Emission data.
• Semi-quantitative analysis capability of unknown samples.
• Fully control of all peripheral units and components (such as Hydride Generator, Autosampler, etc.)
• Upgradability free of charge.

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